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2. PRIMARY CASE STUDIES

2.1 I-90 Near Spearfish, South Dakota (SD-090-019)

Project Description

The South Dakota Department of Transportation (SDDOT) provided this project as a pavement with a history of durability problems. In particular, the pavement is experiencing surface or map cracking over the entire pavement surface. This project represents the primary case study site in the dry-freeze climatic region. The area receives approximately 400 mm of precipitation each year and has a freezing index of 684 °C-days.

This 14-km-long project is located on I-90 near Spearfish, South Dakota and extends from milepost 19.8 to milepost 28.5 in both directions. Table 3-2 provides a summary of the specific design features for this project.

Table 3-2. Summary of design features for SD-090-019.

Category

Design Feature

Description

General
Information

Project limits

MP 19.8 - 28.5

Highway type

Divided

Number of lanes

4

Direction

Eastbound/westbound

Construction date

1968

Cumulative ESALs

~2,250,000

Pavement
Cross Section

Pavement type

JRCP

PCC slab thickness

200 mm

Base

75-mm lime-treated gravel

Subbase

150-mm lime-treated subgrade

Subgrade type

Red clay

Transverse
Joint

Joint spacing

12.3 m

Joint skew

None

Load transfer

25-mm dowels

Sealant type

Silicone

Longitudinal
Joint

Load transfer

 

Sealant type

Hot-pour

Outer
Shoulder

Surface type

AC

Width

3.0 m

Inner
Shoulder

Surface type

AC

Width

1.2 m

Climatic
Conditions

Region

Dry-freeze

Annual precipitation*

400 mm

Freezing index*

684 °C-days

* Climatic data are for Rapid City, South Dakota.

The project is a four-lane divided highway, and the same design was placed in both the eastbound and westbound lanes. It is a jointed reinforced concrete pavement (JRCP) containing wire mesh reinforcement. The joints are spaced at 12.3-m intervals and contain 25-mm dowel bars. The longitudinal centerline joint is sealed with a hot-pour asphalt sealant, whereas the transverse joints are sealed with a silicone sealant. The pavement structure consists of a 200-mm JRCP, a 75-mm lime-treated gravel base, and a 150-mm lime-treated subgrade. The subgrade is a red clayey soil. There are no provisions for subsurface drainage. The inside and outside shoulders are AC-surfaced and are 1.2 and 3.0 m wide, respectively.

Field Evaluation

After an initial investigation, the survey team selected two sections-one each in the inside and outside traffic lanes-to be surveyed in order to evaluate the differences between lanes. Section 001 is located in the eastbound, inside traffic lane beginning at milepost 23.1. This section was constructed in a cut section of approximately 10 m. Section 002 is also located in the eastbound direction but in the outside traffic lane and begins at milepost 24.5. This section was constructed on approximately 3 m of fill material.

A summary of the distress survey results is provided in tables 3-3 and 3-4 for Sections 001 and 002, respectively. Overall, Section 001 appears to be in better structural condition than Section 002, as would be expected due to the lower traffic volumes on the inside traffic lane. Section 001 contains some low-severity transverse cracks, which are expected to occur on JRCP. Spalling occurs at 6 of the 14 transverse joints but only 1 has progressed to medium severity. The spalling appears to be due to the progression of MRD. Three small rigid patches, each of which is located along a transverse joint, are also present. Faulting is virtually nonexistent, averaging 0.6 and 0.7 mm measured at distances of 0.30 and 0.75 m from the slab edge.

Section 002 exhibits more distress and greater deterioration. Although low-severity transverse cracks are expected on JRCP, there are considerably more cracks as compared to Section 001. In addition, Section 002 also exhibits two medium-severity cracks and two high-severity cracks. Faulting is also much more significant, averaging 3.7 and 4.2 mm at 0.30 and 0.75 m from the slab edge. Another distress that is more significant on Section 002 is patching. A high-severity flexible patch is observed, as are 10 low-severity and 2 moderate-severity rigid patches. Some of the rigid patches are full-depth patches at transverse joints, indicating that the joints were likely badly deteriorated at one time. Five of the 14 transverse joints exhibit spalling, including 2 that have progressed to moderate severity.

MRD Field Characterization

During the field surveys, the attributes of the MRD were characterized. Although a definitive diagnosis cannot be made in the field, it is important to evaluate the attributes of the MRD as well as the effect these distresses have on pavement performance. A summary of the MRD characterization for both sections is provided in table 3-5. Figures 3-2 through 3-4 show some the typical conditions observed on the two test sections.

Table 3-3. Summary of pavement condition surveys for SD-090-019-001.

Distress Type

Distress
Measure

Severity Level

Comments

Low

Moderate

High

Cracking

Corner Breaks

number

1

0

0

 

Longitudinal Cracking

linear meters

0.0

0.0

0.0

 

Transverse Cracking

number of cracks

12

0

0

 
 

linear meters

14.7

0.0

0.0

 
 

percent of slabs

0

 

Transverse
Joints

Sealant

 

good condition

silicone sealant

Spalling

number

5

1

0

 
 

linear meters

1.4

0.4

0

 

Faulting

millimeters

0.6

measured at 0.30 m

 

millimeters

0.7

measured at 0.75 m

Width

millimeters

23.6

 

Long. Joints

Sealant

 

fair condition

hot-pour sealant

Spalling

linear meters

0.0

0.0

0.0

 

Shoulder Dropoff

millimeters

17.8

 

Surface
Conditions

Map Cracking

number of slabs

13

all slabs affected

 

square meters

588.3

entire area

Scaling

number of slabs

0

 
 

square meters

0.0

 

Polished Aggregate

square meters

0.0

 

Popouts

number/sq. meter

0.0

 

Other

Blowups

number

0

 

Flexible Patches

number

0

0

0

 
 

square meters

0.0

0.0

0.0

 

Rigid Patches

number

3

0

0

 
 

square meters

0.4

0.0

0.0

 

Pumping/Bleeding

number

0

 
 

linear meters

0.0

 

Table 3-4. Summary of pavement condition surveys for SD-090-019-002.

Distress Type

Distress

Measure

Severity Level

Comments

Low

Moderate

High

Cracking

Corner Breaks

number

1

0

0

 

Longitudinal Cracking

linear meters

0.0

0.0

0.0

 

Transverse Cracking

number of cracks

44

2

2

 
 

linear meters

60.9

7.4

7.4

 
 

percent of slabs

31

 

Transverse
Joints

Sealant

 

good condition

silicone sealant

Spalling

number

3

2

0

 
 

linear meters

1.1

1.9

0.0

 

Faulting

millimeters

3.7

measured at 0.30 m

 

millimeters

4.2

measured at 0.75 m

Width

millimeters

17.2

 

Long. Joints

Sealant

 

fair condition

hot-pour sealant

Spalling

linear meters

0.0

0.0

0.0

 

Shoulder Dropoff

millimeters

23.6

 

Surface
Conditions

Map Cracking

number of slabs

13

all slabs affected

 

square meters

579.0

entire area

Scaling

number of slabs

0

 
 

square meters

0.0

 

Polished Aggregate

square meters

0.0

 

Popouts

number/sq. meter

0.0

 

Other

Blowups

number

0

 

Flexible Patches

number

0

0

1

 
 

square meters

0.0

0.0

0.5

 

Rigid Patches

number

10

2

0

 
 

square meters

15.4

3.8

0.0

 

Pumping/Bleeding

number

0

 
 

linear meters

0.0

 

Table 3-5. Summary of MRD characterization for SD-090-019.

Description

Section 001

Section 002

Comments

Cracking

Location

Entire slab

Entire slab

More significant at slab corners

Orientation/shape

Criss cross

Corners: semi-circle

Center: transverse

 

Extent

Entire slab

Entire slab

 

Crack size

Hairline

Hairline

 

Staining

Location

Joints/cracks

Joints/cracks

 

Color

Brownish gray

Dark gray

 

Exudate

Present

None

Yes

Corners only

Color

n/a

Dark gray/white

 

Extent

n/a

Low

 

Scaling

Location

None

None

 

Area of surface

n/a

n/a

 

Depth

n/a

n/a

 

Vibrator
Trails

Visible

None

None

 

Discolored

n/a

n/a

 

Distressed

n/a

n/a

 

Change in texture

n/a

n/a

 

 Figure 3-2 (a):  Photographs.  Typical distress manifestation observed on SD-090-019-002.  This figure is comprised of two photographs of roadway section 002 and are labeled A and B.  Photograph A shows surface staining along the transverse joint.  Photograph B shows map cracking and spalling along the transverse joint.  Figure 3-2 (b):  Photographs.  Typical distress manifestation observed on SD-090-019-002.  This figure is comprised of two photographs of roadway section 002 and are labeled A and B.  Photograph A shows surface staining along the transverse joint.  Photograph B shows map cracking and spalling along the transverse joint.

(a) Section 002

(b) Section 002


Figure 3-2. Typical distress manifestation observed on SD-090-019-002.

 Figure 3-3 (a):  Photographs.  Typical distress manifestation observed on SD-090-019, Sections 1 and 2.  This figure is comprised of two photographs of roadway labeled A and B.  Photograph A is from section 002 and shows map cracking and spalling along the transverse joint.  The spall has come out and been repaired with an asphalt patch.  Photograph B is from section 001 and shows corner cracking and minor spalling at the intersection of the joints.

 Figure 3-3 (b):  Photographs.  Typical distress manifestation observed on SD-090-019, Sections 1 and 2.  This figure is comprised of two photographs of roadway labeled A and B.  Photograph A is from section 002 and shows map cracking and spalling along the transverse joint.  The spall has come out and been repaired with an asphalt patch.  Photograph B is from section 001 and shows corner cracking and minor spalling at the intersection of the joints.

(a) Section 002

(b) Section 001


Figure 3-3. Typical distress manifestation observed on SD-090-019, Sections 1 and 2.

 Figure 3-4 (a):  Photographs.  Typical distress manifestation observed on SD-090-019-002. This figure is comprised of two photographs of the roadway and are labeled A and B.  Photograph A is a close-up picture of map cracking with secondary material deposits filling the cracks.  A coin has been placed on the ground in the picture to give the viewer perspective.  Photograph B shows corner cracking at the joint intersection along with spalling that has been repaired with a concrete patch.

 Figure 3-4 (b):  Photographs.  Typical distress manifestation observed on SD-090-019-002. This figure is comprised of two photographs of the roadway and are labeled A and B.  Photograph A is a close-up picture of map cracking with secondary material deposits filling the cracks.  A coin has been placed on the ground in the picture to give the viewer perspective.  Photograph B shows corner cracking at the joint intersection along with spalling that has been repaired with a concrete patch.

(a)

(b)


Figure 3-4. Typical distress manifestation observed on SD-090-019-002.

On both pavement sections, map cracking was observed throughout the entire area. On Section 001, the cracks appear to be confined to the upper 50 mm at the pavement surface. The majority of cracks run perpendicular to the centerline, but there are some cracks that run parallel to the centerline. The combination of cracks forms a criss-cross pattern on the surface. Although the cracking pattern is similar on Section 002, the transverse cracks on Section 001 are more pronounced and some are opened at the surface.

On Section 001, the area around the joints is discolored, showing a brownish-gray staining. However, the cracking pattern around the joints is similar to the slab interior. The MRD has progressed at a few of the slab corners and spalling has occurred. There is no exudate from the cracks on this section.

Section 002 exhibits a different cracking pattern along the joints. The cracking and staining form a semi-circular pattern, widening at the slab corners. A dark gray staining is observed around both the longitudinal and transverse joints. Unlike Section 001, exudate is observed at some cracks, particularly cracks located near a joint. The exudate is either a dark gray or white substance.

Laboratory Analysis

Core Selection/Visual Inspection

Based upon the field survey, distress was detected at joints and near slab corners. Photos of typical distresses are shown in figure 3-5. To look at concrete from more than one slab, Cores B and D were selected from Section 001 and Cores A, B, and C were selected from Section 002. All cores were cut to produce slabs for examination with stains.

 Figure 3-5 (a):  Photographs.  Core specimens from SD-090-019.  This figure is comprised of three photographs labeled A, B, and C.  Photograph A is of a slab from section 001, core B.  The core was taken from the transverse joint and shows evidence of spalling as there is some material missing from the top of the slab.  Photograph B is a picture of core specimen SD090002A and is from section 001.  The core was taken from the transverse joint area and has a steel dowel bar running through the center of it.  The core was taken from the road surface to a depth of 19 centimeters.  Photograph C is a picture of core specimen SD090002C and is from section 001.  The core also is taken from the road surface to a depth of 19 centimeters.  A thin crack can be seen running through the bottom third of the core.

 

 Figure 3-5 (b):  Photographs.  Core specimens from SD-090-019.  This figure is comprised of three photographs labeled A, B, and C.  Photograph A is of a slab from section 001, core B.  The core was taken from the transverse joint and shows evidence of spalling as there is some material missing from the top of the slab.  Photograph B is a picture of core specimen SD090002A and is from section 001.  The core was taken from the transverse joint area and has a steel dowel bar running through the center of it.  The core was taken from the road surface to a depth of 19 centimeters.  Photograph C is a picture of core specimen SD090002C and is from section 001.  The core also is taken from the road surface to a depth of 19 centimeters.  A thin crack can be seen running through the bottom third of the core.

 

 Figure 3-5 (c):  Photographs.  Core specimens from SD-090-019.  This figure is comprised of three photographs labeled A, B, and C.  Photograph A is of a slab from section 001, core B.  The core was taken from the transverse joint and shows evidence of spalling as there is some material missing from the top of the slab.  Photograph B is a picture of core specimen SD090002A and is from section 001.  The core was taken from the transverse joint area and has a steel dowel bar running through the center of it.  The core was taken from the road surface to a depth of 19 centimeters.  Photograph C is a picture of core specimen SD090002C and is from section 001.  The core also is taken from the road surface to a depth of 19 centimeters.  A thin crack can be seen running through the bottom third of the core.

(a) Section 001, Core B

 

(b) Section 002, Core A

 

(c) Section 002, Core C

Figure 3-5. Core specimens from SD-090-019.

Mix proportions were estimated by inspecting the cores visually before and after slicing. In this case, detailed construction records were unavailable to verify the mix design. The concrete was well consolidated with no apparent segregation or parallelism of the aggregates. No scaling or sub-parallel cracking was apparent on these sites. The embedded steel was at a sufficient depth to prevent corrosion and no entrapped water voids were seen under aggregates or embedded steel. Surface cracking was apparent that was not related to plastic shrinkage cracking.

Stereo Optical Microscopy

The stereo optical microscope was used to first examine polished slabs cut from each core to assess the general condition of the concrete. Typical micrographs of interesting features are presented in figures 3-6 and 3-7. The aggregate type was determined to be a natural gravel with a varied lithology including limestone, siltstone, dolomite, and rhyolite as the main rock types for the coarse aggregate. Many of the rhyolite particles had small feldspar inclusions. The fine aggregates contained the same rock types seen in the coarse aggregate in addition to shale, sandstone quartzite, and granite. Cracks passing through the paste also passed through aggregates. Reaction rims were visible along with secondary infilling in cracks and air voids. A yellow to white "soft" crumbly siltstone constituent of the coarse aggregate natural gravel is frequently cracked, with the cracks extending into the surrounding cement paste, and occasional white deposits in cracks. Aggregate particles that were volcanics or rhyolites appear to be reactive.

 Figure 3-6 (a):  Photographs.  Stereo optical micrographs of typical cracking pattern associated with porous siltstone aggregate SD-090-019.  This figure is comprised of two photographs labeled A and B.  Photograph A is a micrograph of the siltstone aggregate. Cracking is seen running through and around the aggregate particles.  Multiple open air voids also are visible in the micrograph.  Photograph B is a micrograph of the siltstone and rhyolite aggregate.  Cracking is seen running through the aggregate and into the paste.  The aggregate rims are also visible on several of the larger particles as are several open air voids.

 

 Figure 3-6 (b):  Photographs.  Stereo optical micrographs of typical cracking pattern associated with porous siltstone aggregate SD-090-019.  This figure is comprised of two photographs labeled A and B.  Photograph A is a micrograph of the siltstone aggregate. Cracking is seen running through and around the aggregate particles.  Multiple open air voids also are visible in the micrograph.  Photograph B is a micrograph of the siltstone and rhyolite aggregate.  Cracking is seen running through the aggregate and into the paste.  The aggregate rims are also visible on several of the larger particles as are several open air voids.

(a) Siltstone aggregate

 

(b) Siltstone and rhyolite aggregate


Figure 3-6. Stereo optical micrographs of typical cracking pattern associated with porous siltstone aggregate SD-090-019.

 Figure 3-7 (a):  Photographs.  Stereo optical micrograph showing gel deposits in SD-090-019 aggregates.  This figure is comprised of two photographs labeled A and B.  Photograph A is a micrograph of the metamorphic aggregate.  The micrograph is centered on one large piece of aggregate that has a large crack running through it.  Photograph B is a micrograph of the siltstone aggregate.  Cracking can be seen running through the aggregate.  Several areas in the paste appear bright white in color, which is caused by reaction products in the paste.

 

 Figure 3-7 (b):  Photographs.  Stereo optical micrograph showing gel deposits in SD-090-019 aggregates.  This figure is comprised of two photographs labeled A and B.  Photograph A is a micrograph of the metamorphic aggregate.  The micrograph is centered on one large piece of aggregate that has a large crack running through it.  Photograph B is a micrograph of the siltstone aggregate.  Cracking can be seen running through the aggregate.  Several areas in the paste appear bright white in color, which is caused by reaction products in the paste.

(a) Metamorphic aggregate

 

(b) Siltstone aggregate


Figure 3-7. Stereo optical micrograph showing gel deposits in SD-090-019 aggregates.

The stereo microscope was also used to perform a modified point count in accordance with ASTM C 457. As part of the modified point count, the volume fractions of paste and aggregate were also determined to confirm mix volumetrics. The results of this analysis are given in table 3-6.

Table 3-6. Results of ASTM C 457 for concrete from SD-090-019.

 

Original

Existing

Volume Percent

Core

Air Content
(vol. %)

Spacing Factor
(mm)

Air Content
(vol. %)

Spacing Factor
(mm)

Paste
(vol. %)

Coarse Aggregate
(vol. %)

Fine Aggregate
(vol. %)

Site 1 Core A

6.0

0.1274

6.0

0.1375

25.6

47.9

20.5

Site 1 Core D

5.7

0.1073

5.7

0.1047

26.4

52.0

15.9

Site 2 Core C

5.5

0.1089

5.4

0.1114

27.16

41.5

25.8

Staining Tests

The sodium cobaltinitrite/rhodamine B staining tests were applied and a number of aggregates were identified as being susceptible to alkali-silica reactivity (ASR). The phenolphthalein staining method was used to determine the depth of carbonation on freshly cut surfaces. Slabs cut from the analyzed cores were tested for depth of carbonation with no core having a depth of carbonation greater than 2 mm below the road surface. Barium chloride/potassium permanganate stain was used to identify sulfate minerals. Examples of the stained slabs are presented in figures 3-8 through 3-11.

 Figure 3-8 (a):  Photographs.  Slab 1B stained with sodium cobaltinitrite/rhodamine B from SD-090-019-001.  This figure is comprised of three photographs of slab 1B labeled A, B, and C.  The slab was stained with sodium cobaltinitrite/rhodamine B.  Photograph A is a picture of stained slab 1B, which is cracked at the bottom.  Photograph B is a stereo optical micrograph of a reactive porous siltstone particle from slab 1B. Internal cracking can be seen in the aggregate particle.  Photograph C is a stereo optical micrograph of a reactive volcanic particle.  Internal cracking can also be seen in this picture running through the aggregate particle.  Several areas in and around the aggregate particle appear white in color, which could be caused by reaction products, although this is not certain

 

 Figure 3-8 (b):  Photographs.  Slab 1B stained with sodium cobaltinitrite/rhodamine B from SD-090-019-001.  This figure is comprised of three photographs of slab 1B labeled A, B, and C.  The slab was stained with sodium cobaltinitrite/rhodamine B.  Photograph A is a picture of stained slab 1B, which is cracked at the bottom.  Photograph B is a stereo optical micrograph of a reactive porous siltstone particle from slab 1B. Internal cracking can be seen in the aggregate particle.  Photograph C is a stereo optical micrograph of a reactive volcanic particle.  Internal cracking can also be seen in this picture running through the aggregate particle.  Several areas in and around the aggregate particle appear white in color, which could be caused by reaction products, although this is not certain

(b) Stereo optical micrograph of reactive porous siltstone particle

 Figure 3-8 (c):  Photographs.  Slab 1B stained with sodium cobaltinitrite/rhodamine B from SD-090-019-001.  This figure is comprised of three photographs of slab 1B labeled A, B, and C.  The slab was stained with sodium cobaltinitrite/rhodamine B.  Photograph A is a picture of stained slab 1B, which is cracked at the bottom.  Photograph B is a stereo optical micrograph of a reactive porous siltstone particle from slab 1B. Internal cracking can be seen in the aggregate particle.  Photograph C is a stereo optical micrograph of a reactive volcanic particle.  Internal cracking can also be seen in this picture running through the aggregate particle.  Several areas in and around the aggregate particle appear white in color, which could be caused by reaction products, although this is not certain

(a) Stained slab

 

(c) Stereo optical micrograph of reactive volcanic particle

Figure 3-8. Slab 1B stained with sodium cobaltinitrite/rhodamine B from SD-090-019-001.

 Figure 3-9 (a):  Photographs.  Slab 1B stained with sodium cobaltinitrite/rhodamine B from SD-090-019-001.  This figure is comprised of two photographs of slab 1B labeled A and B.  The slab was stained with sodium cobaltinitrite/rhodamine B.  Photograph A is a picture of the entire stained slab.  A large crack is visible approximately half way down the slab.  Photograph B is a stereo optical micrograph of a reactive rhyolite particle.  The particle has a crack running it and reactive materials are visible in the paste surrounding the particle.  The figure also contains a table listing the litho types, their volume in milliliters and their volume as a percent of total volume.  Volume was determined by water displacement from a sample gathered at a nearby river.  The total volume of all of the lithos was 1,479 milliliters.  The information in the table is as follows:

 

(b) Stereo optical micrograph of reactive rhyolite particle

(a) Stained slab

 

(c)

Figure 3-9. Slab 1B stained with sodium cobaltinitrite/rhodamine B from SD-090-019-001.

 Figure 3-10 (a):  Photographs.  Slab 2B stained with sodium cobatinitrite/rhodamine B from SD-090-019-002.  This figure is comprised of four photographs of slab 2B, labeled A, B, C, and D.  The slab was stained with cobaltinitrite/rhodamine B. Photograph A is a picture of the entire stained slab.  The slab is cracked on the left hand side, but this possibly resulted when the slab was being cut.  Photograph B is of a reactive aggregate particle found in the slab.  Photograph C is a picture of an ASR gel filled void that abuts a larger aggregate particle.  Reaction rims are visible around the aggregate.  Photograph D is of a reactive aggregate particle.

 

 Figure 3-10 (b):  Photographs.  Slab 2B stained with sodium cobatinitrite/rhodamine B from SD-090-019-002.  This figure is comprised of four photographs of slab 2B, labeled A, B, C, and D.  The slab was stained with cobaltinitrite/rhodamine B. Photograph A is a picture of the entire stained slab.  The slab is cracked on the left hand side, but this possibly resulted when the slab was being cut.  Photograph B is of a reactive aggregate particle found in the slab.  Photograph C is a picture of an ASR gel filled void that abuts a larger aggregate particle.  Reaction rims are visible around the aggregate.  Photograph D is of a reactive aggregate particle.

(a) Stained slab

 

(b) Reactive aggregate particle

 Figure 3-10 (c):  Photographs.  Slab 2B stained with sodium cobatinitrite/rhodamine B from SD-090-019-002.  This figure is comprised of four photographs of slab 2B, labeled A, B, C, and D.  The slab was stained with cobaltinitrite/rhodamine B. Photograph A is a picture of the entire stained slab.  The slab is cracked on the left hand side, but this possibly resulted when the slab was being cut.  Photograph B is of a reactive aggregate particle found in the slab.  Photograph C is a picture of an ASR gel filled void that abuts a larger aggregate particle.  Reaction rims are visible around the aggregate.  Photograph D is of a reactive aggregate particle.

 

 Figure 3-10 (d):  Photographs.  Slab 2B stained with sodium cobatinitrite/rhodamine B from SD-090-019-002.  This figure is comprised of four photographs of slab 2B, labeled A, B, C, and D.  The slab was stained with cobaltinitrite/rhodamine B. Photograph A is a picture of the entire stained slab.  The slab is cracked on the left hand side, but this possibly resulted when the slab was being cut.  Photograph B is of a reactive aggregate particle found in the slab.  Photograph C is a picture of an ASR gel filled void that abuts a larger aggregate particle.  Reaction rims are visible around the aggregate.  Photograph D is of a reactive aggregate particle.

(c) ASR gel filled void

 

(d) Reactive aggregate particle

Figure 3-10. Slab 2B stained with sodium cobaltinitrite/rhodamine B from SD-090-019-002.

 Figure 3-11 (a):  Photographs.  Stereo optical micrographs of air voids filled with sulfate minerals stained with potassium permanganate.  (Note differences due to polishing.)  This figure is comprised of four photographs labeled A, B, C, and D.  Photographs A and B are of ettringite filled voids on polished surfaces.  Photograph A focuses on one filled-void, while photograph B shows at least two filled voids.  The ettringite filled voids are much more evident in Photograph B than A.  Photographs C and D are images of an unpolished surface, both showing air voids filled with sulfate materials.  All air voids appear to be filled in Photographs C and D.

 

 Figure 3-11 (b):  Photographs.  Stereo optical micrographs of air voids filled with sulfate minerals stained with potassium permanganate.  (Note differences due to polishing.)  This figure is comprised of four photographs labeled A, B, C, and D.  Photographs A and B are of ettringite filled voids on polished surfaces.  Photograph A focuses on one filled-void, while photograph B shows at least two filled voids.  The ettringite filled voids are much more evident in Photograph B than A.  Photographs C and D are images of an unpolished surface, both showing air voids filled with sulfate materials.  All air voids appear to be filled in Photographs C and D.

(a) Ettringite filled voids on polished surface

 

(b) Ettringite filled voids on polished surface

 Figure 3-11 (c):  Photographs.  Stereo optical micrographs of air voids filled with sulfate minerals stained with potassium permanganate.  (Note differences due to polishing.)  This figure is comprised of four photographs labeled A, B, C, and D.  Photographs A and B are of ettringite filled voids on polished surfaces.  Photograph A focuses on one filled-void, while photograph B shows at least two filled voids.  The ettringite filled voids are much more evident in Photograph B than A.  Photographs C and D are images of an unpolished surface, both showing air voids filled with sulfate materials.  All air voids appear to be filled in Photographs C and D.

 

 Figure 3-11 (d):  Photographs.  Stereo optical micrographs of air voids filled with sulfate minerals stained with potassium permanganate.  (Note differences due to polishing.)  This figure is comprised of four photographs labeled A, B, C, and D.  Photographs A and B are of ettringite filled voids on polished surfaces.  Photograph A focuses on one filled-void, while photograph B shows at least two filled voids.  The ettringite filled voids are much more evident in Photograph B than A.  Photographs C and D are images of an unpolished surface, both showing air voids filled with sulfate materials.  All air voids appear to be filled in Photographs C and D.

(c) Ettringite filled voids on unpolished surface

 

(d) Ettringite filled voids on unpolished surface


Figure 3-11. Stereo optical micrographs of air voids filled with sulfate minerals stained with potassium permanganate (note differences due to polishing).

Petrographic Optical Microscopy

Based upon stereo microscope observations and staining, thin sections were prepared from the selected cores. Surfaces were sectioned from the core adjacent to stained sections to avoid contamination from the stains. The reactive coarse aggregates were primarily the siltstones and rhyolites, although others were noted as reactive. The shale was commonly associated with ASR in fine aggregate. In addition to cracking associated with ASR, other cracking of non-reacted siltstone aggregates was noted. The siltstone aggregates had a very porous microstructure as seen in thin section. These aggregates may be susceptible to aggregate freeze-thaw deterioration, leading to some of the cracking seen in the concrete. In addition to possible ASR and aggregate freeze-thaw deterioration, evidence of alkali-carbonate reactivity (ACR) was noted where densified paste regions or "halos" with a large amount of calcite were seen surrounding dolomite coarse aggregates (Spry et al. 1996). Secondary deposits within cracks and voids were identified. In addition to specific phases identified (e.g., ASR gel, calcite), ettringite was common as a secondary deposit. In addition to these diagnostic features, hydrocalumite (Friedel's salt) secondary deposits were found. Given the high chloride concentration needed to precipitate hydrocalumite, this is taken as a diagnostic feature of deicer attack. Petrographic micrographs are presented in figures 3-12 and 3-13.

 Figure 3-12:  Photographs.  Core SD-090-019-001B, thin-section micrographs of same rhyolite aggregate that was stained with cobaltinitrite ASR stained as shown in Figure 3-9 B.  This figure is comprised of three micrographs, each taken using a different light.  The top micrographs used a transmitted plan polarized light, the middle micrograph was taken in the epifluorescent mode, and the bottom micrograph used a transmitted cross polarized light.  All three show the interface between an aggregate particle and the paste.  In the micrographs, ettringite can be seen filling the entrained air void, ASR gel can be seen in the crack within the aggregate, and hydrocalumite can be seen in the crack along the contact area between the aggregate and the cement paste.  This same area was analyzed with the SEM to collect quantitative chemical information about the gel, ettringite, and hydrocalumite.  The micrographs represent 90 times magnification.

Figure 3-12. Core SD-090-019-001B, thin-section micrographs of same rhyolite aggregate that was stained with sodium cobaltinitrite ASR stain as shown in figure 3-9 (b).

From top to bottom: transmitted plane polarized light, epifluorescent mode, and transmitted cross polarized light. Ettringite can be seen filling the entrained air void, ASR gel can be seen in the crack within the aggregate, and hydrocalumite can be seen in the crack along the contact between the aggregate and the cement paste. This same area was analyzed with the SEM to collect quantitative chemical information about the gel, ettringite, and hydrocalumite.

90x magnification

 Figure 3-13:  Photographs.  Core SD-090-019-001B, thin section micrographs of the same volcanic aggregate that was stained with sodium cobatinitrite ASR stain as shown in Figure 3-8 C.  This figure is comprised of three micrographs, each taken using a different light.  The top micrographs used a transmitted plan polarized light, the middle micrograph was taken in the epifluorescent mode, and the bottom micrograph used a transmitted cross polarized light.  All three show the interface between an aggregate particle and the paste.  In the micrographs, ettringite can be seen filling the entrained air void.  ASR gel can be seen in the crack within the aggregate.  This crack runs through the aggregate and into the paste and through an air void.  This is most evident in the micrograph taken in epifluorescent mode.  Also, hydrocalumite can be seen in the small entrained air void in the lower right hand corner.  This same area was analyzed with the scanning electron microscope to collect quantitative chemical information about the gel, ettringite, and hydrocalumite.  The micrographs represent 90 times magnification.

Figure 3-13. Core SD-090-019-001B, thin-section micrographs of same volcanic aggregate that was stained with sodium cobaltinitrite ASR stain as shown in figure 3-8 (c).

From top to bottom: transmitted plane polarized light, epifluorescent mode, and transmitted cross polarized light. Ettringite can be seen filling the entrained air void, ASR gel can be seen in the crack within the aggregate, and hydrocalumite can be seen in the small entrained air void in the lower right hand corner. This same area was analyzed with the SEM to collect quantitative chemical information about the gel, ettringite, and hydrocalumite.

90x magnification

Scanning Electron Microscopy (SEM)

A conventional SEM was used to identify secondary deposits seen in the petrographic microscope examination to confirm those observations. Figure 3-14 containsa backscattered electron image showing an ettringite filled void, a crack filled with hydrocalumite, and characteristic x-ray spectra from each phase illustrating their compositions. The SEM analysis confirmed the petrographic analysis with regards to the composition of the secondary deposits. The phase identified as hydrocalumite was confirmed, as were the presence of ettringite and the composition of various ASR reaction products. The results of x-ray microanalyses of the ettringite and the hyrocalumite phases are presented in tables 3-7 and 3-8, respectively. Figure 3-15 presents the ternary diagram showing the probable range of composition for the hydrocalumite deposits.

 Figure 3-14 (a):  Photographs.  Ettringite in A and hydrocalumite in B infilling in void and crack, respectively.  Example spectra from each phase shown in C and D.  This figure is comprised of four photographs.  Photograph A contains a backscattered electron image of ettringite filling a void.  ASR gel also can be seen filling a crack running through the aggregate particle.  Photograph B contains a backscattered electron image of a crack filled with hydrocalumite.  Photograph C is a spectrum showing that the secondary fill material in the air void is ettringite as the three peaks on the spectrum indicate the presence of aluminum, calcium, and sulfur.  Photograph D is a spectrum from the analysis of the material that is filling the crack in Photograph B.  It is evident that this material is hydrocalumite, as the peaks on the spectrum indicate the presence of aluminum and calcium.   Figure 3-14 (b):  Photographs.  Ettringite in A and hydrocalumite in B infilling in void and crack, respectively.  Example spectra from each phase shown in C and D.  This figure is comprised of four photographs.  Photograph A contains a backscattered electron image of ettringite filling a void.  ASR gel also can be seen filling a crack running through the aggregate particle.  Photograph B contains a backscattered electron image of a crack filled with hydrocalumite.  Photograph C is a spectrum showing that the secondary fill material in the air void is ettringite as the three peaks on the spectrum indicate the presence of aluminum, calcium, and sulfur.  Photograph D is a spectrum from the analysis of the material that is filling the crack in Photograph B.  It is evident that this material is hydrocalumite, as the peaks on the spectrum indicate the presence of aluminum and calcium.
 Figure 3-14 (c):  Photographs.  Ettringite in A and hydrocalumite in B infilling in void and crack, respectively.  Example spectra from each phase shown in C and D.  This figure is comprised of four photographs.  Photograph A contains a backscattered electron image of ettringite filling a void.  ASR gel also can be seen filling a crack running through the aggregate particle.  Photograph B contains a backscattered electron image of a crack filled with hydrocalumite.  Photograph C is a spectrum showing that the secondary fill material in the air void is ettringite as the three peaks on the spectrum indicate the presence of aluminum, calcium, and sulfur.  Photograph D is a spectrum from the analysis of the material that is filling the crack in Photograph B.  It is evident that this material is hydrocalumite, as the peaks on the spectrum indicate the presence of aluminum and calcium.  Figure 3-14 (d):  Photographs.  Ettringite in A and hydrocalumite in B infilling in void and crack, respectively.  Example spectra from each phase shown in C and D.  This figure is comprised of four photographs.  Photograph A contains a backscattered electron image of ettringite filling a void.  ASR gel also can be seen filling a crack running through the aggregate particle.  Photograph B contains a backscattered electron image of a crack filled with hydrocalumite.  Photograph C is a spectrum showing that the secondary fill material in the air void is ettringite as the three peaks on the spectrum indicate the presence of aluminum, calcium, and sulfur.  Photograph D is a spectrum from the analysis of the material that is filling the crack in Photograph B.  It is evident that this material is hydrocalumite, as the peaks on the spectrum indicate the presence of aluminum and calcium.

Figure 3-14. Ettringite (a) and hydrocalumite (b) infilling in void and crack, respectively. Example spectra from each phase are shown in (c) and (d), respectively.

Table 3-7. Summary of 10 analyses from ettringite deposits, compared to a calculated composition for dehydrated ettringite.

Element

Average
Wt. %

Standard
Deviation

Dehydrated
Ettringite

Na

0.2

0.2

0.0

Mg

0.0

0.0

0.0

Al

7.9

0.3

6.9

Si

0.3

0.1

0.0

S

11.6

0.5

12.2

Cl

0.2

0.1

0.0

K

0.0

0.0

0.0

Ca

31.2

0.6

30.6

Ti

0.0

0.0

0.0

Mn

0.0

0.1

0.0

Fe

0.0

0.1

0.0

O

-

-

48.8

H

-

-

1.5

sum

51.3

 

100.0


Table 3-8. Summary of 13 analyses from hydrocalumite deposits, compared to calculated compositions for the 3 dehydrated end members of the hydrocalumite solid solution series.

Element

Average
Wt. %

Standard
Deviation

Dehydrated
Cl- hydrocalumite

Dehydrated OH- hydrocalumite

Dehydrated
CO3-2 hydrocalumite

Na

0.0

0.1

0.0

0.0

0.0

Mg

0.0

0.1

0.0

0.0

0.0

Al

12.5

0.4

11.0

12.9

12.5

Si

0.4

0.4

0.0

0.0

0.0

S

0.0

0.0

0.0

0.0

0.0

Cl

5.0

0.2

14.5

0.0

0.0

K

0.0

0.1

0.0

0.0

0.0

Ca

36.0

0.8

32.8

38.3

37.3

Ti

0.0

0.0

0.0

0.0

0.0

Mn

0.0

0.1

0.0

0.0

0.0

Fe

0.3

0.2

0.0

0.0

0.0

C

-

-

0.0

0.0

2.8

 

-

-

39.2

45.9

44.6

H

-

-

2.5

2.9

2.8

sum

54.2

 

100.0

100.0

100.0


 Figure 3-15:  Diagram.  Ternary diagram showing the probable range of composition for the hydrocalumite.  This diagram shows a triangle with chemical compounds labeling each of three corners. The triangle's lower left corner is labeled with a hydrocalumite formula that contains a hydroxide molecule.  The triangle's right hand corner is labeled with a hydrocalumite formula that contains carbonate.  Finally, the top of the triangle is labeled as hydrocalumite containing chlorine.  According to the diagram, the probably range of composition for the hydrocalumite from the analysis is somewhere between or something similar to these three other types of hydrocalumite.

Figure 3-15. Ternary diagram showing the probable range of composition for the hydrocalumite deposits analyzed from SD-090-019.

Chemical Laboratory Tests

Ion chromatography was used to analyze the sulfate content of soil samples taken from the grade below the individual core holes. The complete analysis is presented in the final report. To summarize, the soil base below the test sites would be classified as a negligible sulfate exposure using the criteria set forth in ACI 201.2R-92 Guides to Durable Concrete.

Interpretation and Diagnosis

Having performed the described laboratory analyses and applied the diagnostic flowcharts as shown in figures 3-16 through 3-20, several possible MRDs were identified in SD-090-019-001, including ASR, ACR, aggregate freeze-thaw, and deicer attack. This is consistent with the visual observations of the distress reported from the field where mixtures of diagnostic features were apparent. To finalize the diagnosis, the diagnostic tables were consulted. The diagnostic features identified in the analysis processes are listed below in table 3-9 along with their associated MRD type and significance as related to this pavement. A brief discussion follows of each possible MRD identified in the laboratory analysis:

ASR - This MRD seems to be the most dominant given its extent in the sections sampled. From the standpoint of the guidelines, all diagnostic features of ASR were present with the exception of known poor performance for the aggregate used.

ACR - This MRD was identified as a possible but in the final analysis is not listed as probable as a major contributor. Although there was strong evidence of the reactivity of some dolomite aggregates, the extent and magnitude of this reaction was not great.

Aggregate Freeze-Thaw - Like ASR, this appeared to be a dominant distress in terms of extent. The likelihood or certainty of diagnosis is also very high given that, with the exception of known poor performance for the aggregate used, 75 percent of all diagnostic features for aggregate freeze-thaw were present.

Deicer Attack - This MRD is probably the most difficult to diagnose as it can often be present and hidden by other MRDs. The key diagnostic feature that makes deicer attack probable is the occurrence of hydrocalumite as an infilling material in cracks and voids.

As stated previously, it is not rare to find a pavement with diagnostic features representative of more than one distress mechanism present. In most of these cases, as with this one, the failure of the concrete cannot be attributed to one particular cause. However, in this case some general observations can be made. First, the ASR, aggregate freeze-thaw, and potential ACR distresses may not have occurred if a higher quality aggregate source was used. As is most often the case, contractors use the best possible aggregate source economically feasible but in some locations, such as central South Dakota, the possibilities are limited. The other distress mechanism identified, deicer attack, is more problematic as deicers are clearly required on this portion of the interstate system. A lower water-to-cement ratio (w/c) would likely reduce the concrete permeability and thus reduce the likelihood of a recurrence of this distress.

Recommended Treatment/Rehabilitation Alternatives

Using the procedures presented in Guideline III in Volume 2: Guidelines Description and Uses, feasible treatment and rehabilitation alternatives were selected. The two most significant MRD mechanisms found were aggregate freeze-thaw deterioration and ASR. Because the two mechanisms are acting in concert, it is difficult to rate the severity of each independently, but the level of spalling and patching at the transverse joints indicates that the severity level is likely a medium severity in Section 001 and medium to high in Section 002. The extent was at both joints and cracks and at corners. As a result, feasible treatment/rehabilitation alternatives include:

The use of patching is still feasible even though ASR was observed since most deterioration is isolated in the vicinity of joints and cracks. Further, lithium compounds are not suggested since they are ineffective in delaying aggregate freeze-thaw damage.

Ultimately, as the pavement continues to deteriorate, a reconstruction/recycling option becomes more viable. If recycling is considered, precautions must be taken to avoid aggregate freeze-thaw deterioration and/or ASR in the newly constructed pavement.

   Figure 3-16:  Flowchart.  Flowchart for assessing the likelihood of MRD causing the observed distress in the pavement as applied to the Spearfish, South Dakota site.  This flowchart is used to determine whether pavement distress is actually an MRD and whether a visual inspection and examination of the paste and aggregate should occur.  By evaluating field and maintenance surveys and using this flowchart from Volume 2 of the guidelines, evidence was found that showed that the problem at the Spearfish site was a possible MRD because cracking was found to be present and concentrated at and parallel to the joints.

Figure 3-16. Flowchart for assessing the likelihood of MRD causing the observed distress in the pavement as applied to the Spearfish, South Dakota site.


Possible Distress

Present

Additional Information

Error in Mix Proportioning

Yes

No

See Recommended Literature

Poor Placement

Yes

No

See Recommended Literature

Poor Finishing/Curing

Yes

No

See Recommended Literature

Poor Steel Placement

Yes

No

See Recommended Literature

Carbonation at Depths > 5-10 mm

Yes

No

See Recommended Literature


Figure 3-17. Click for explanation of the figure

Figure 3-17. Flowchart for assessing general concrete properties based on visual examination as applied to the Spearfish, South Dakota site.

 Click on the diagram for explanation

Figure 3-18. Flowchart for assessing the condition of the concrete paste as applied to the Spearfish, South Dakota site.


Possible Distress

Present

Additional Information

Natural Cracking of Aggregate

Yes

No

See Recommended Literature

Sample Preparation Cracks

Yes

No

See Recommended Literature

Aggregate Freeze Thaw

Yes

No

Table II-3

Natural Weathering of Aggregates

Yes

No

See Recommended Literature

Alkali Silica Reaction

Yes

No

Table II-6

Alkali Carbonate Reaction

Yes

No

Table II-7

Secondary Deposits

Yes

No

Figure 3-20

Figure 3-19. Click for explanation of the figure

Figure 3-19. Flowchart for assessing the condition of the concrete aggregates as applied to the Spearfish, South Dakota site.


Possible Distress

Present

Additional Information

Sulfate Attack

Yes

No

Table II-4

Deicer Attack

Yes

No

Table II-5

Alkali Silica Reaction

Yes

No

Table II-6

Alkali Carbonate Reaction

Yes

No

Table II-7

Corrosion of Embedded Steel

Yes

No

Table II-1

Figure 3-20. Click for explanation of the figure

Figure 3-20. Flowchart for identifying infilling materials in cracks and voids as applied to the Spearfish, South Dakota site.


Table 3-9. Identified diagnostic features along with their associated MRD type and significance as related to SD-090-019.

Diagnostic
Feature

Method of Characterization

Associated with MRD Type

Significance

Secondary deposits filling air voids

Staining
Stereo OM
Petrographic OM
SEM

Paste freeze-thaw, deicer attack, ASR, ACR, Sulfate attack (both internal and external)

Low

Staining at joints or cracks

Field evaluation

Deicer attack

Moderate

Secondary deposits of chloroaluminates

Petrographic OM
SEM

High

Cracking near joints/cracks

Field evaluation

Aggregate freeze-thaw

Moderate

Staining/Spalling

Field evaluation

Moderate

Cracks through non-reactive coarse aggregates

Visual inspection
Stereo OM
Petrographic OM
SEM

High

Poor void structure in the aggregate

Petrographic OM
CSEM
LVSEM

High

Map Cracking with exudate

Visual inspection

ASR

High

ASR reaction product in cracks and voids

Stereo OM
Petrographic OM

High

Reaction rims on aggregates

Visual inspection
Stereo OM
Petrographic OM
SEM

Moderate

Microcracking radiating from reacted cracked aggregate

Stereo OM
Petrographic OM
SEM

High

Map Cracking

Field evaluation

Sulfate attack

Moderate

Significant sulfate deposits in cracks and voids

Staining
Stereo OM
Petrographic OM
SEM

Low

Recommended Prevention Strategies

For the distresses noted, the best preventative strategy is to use a different source of aggregate. Testing in accordance with the guidelines should show that the current source would be unacceptable without mitigation. Mitigation strategies for aggregate freeze-thaw deterioration that could be used if current aggregate source is all that is available include:

To address the potential for ASR, the following strategies can be employed to reduce the reactivity of the aggregate:

If aggregate benefaction is not feasible or cost effective, other strategies can also be employed including:

Regardless of the approach, the design PCC mixture must be tested to ensure that the aggregate freeze-thaw deterioration and ASR have been mitigated.

2.2 TH 65 in Mora, Minnesota (MN-065-064)

Project Description

The Minnesota DOT provided several candidate projects with durability problems. One of the projects-located on TH 65 in downtown Mora-was experiencing severe durability problems concentrated at the transverse joints. This project was selected as the primary case study site for the wet-freeze climatic region. This area receives approximately 660 mm of annual precipitation and has a freezing index of 1030 °C-days.

Table 3-10 presents a summary of the design information for this project. This project extends from milepost 64.2 to 65.0 and is located in both the northbound and southbound lanes. It is a four-lane divided roadway separated by a concrete median; some sections also include an additional lane for left-turn traffic. The pavement, which was constructed in 1989, consists of a 200-mm jointed plain concrete pavement (JPCP) with a 75-mm granular base and a 305-mm granular subbase. The transverse joints are skewed and have a variable joint spacing pattern of 4.0-4.6-5.2-4.6 m. Load transfer is provided by aggregate interlock only; no additional load transfer devices have been employed. The only variation in the two sections is the transverse joint sealant-Section 001 uses silicone sealant and Section 002 uses hot-pour sealant. The longitudinal joints are not sealed. A 2.4-m-wide AC shoulder is placed at the outer edge; there is no inside shoulder due to the concrete median.

Table 3-10. Summary of design features for MN-065-064.

Category

Design Feature

Description

General Information

Project limits

MP 64.2 - 65.0

Highway type

Divided

Number of lanes

4

Direction

Northbound/southbound

Construction date

1989

Cumulative ESALs

~300,000

Pavement
Cross Section

Pavement type

JPCP

PCC slab thickness

200 mm

Base

75-mm granular

Subbase

305-mm granular

Subgrade type

Unknown

Transverse
Joint

Joint spacing

4.0-4.6-5.2-4.6 m

Joint skew

1:12

Load transfer

Aggregate interlock

Sealant type

Silicone (001); hot-pour (002)

Longitudinal
Joint

Load transfer

 

Sealant type

None

Outer
Shoulder

Surface type

AC

Width